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One-Pot Three-Step Synthesis of Naphtho[2,3- a ]carbazole- 5,13-diones using a Tandem Radical Alkylation-Cyclization- Aromatization Reaction Sequence

One-Pot Three-Step Synthesis of Naphtho[2,3- a ]carbazole- 5,13-diones using a Tandem Radical Alkylation-Cyclization- Aromatization Reaction Sequence,

One-Pot Three-Step Synthesis of Naphtho[2,3- a ]carbazole- 5,13-diones using a Tandem Radical Alkylation-Cyclization- Aromatization Reaction Sequence   (Citations: 2)
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    • ...naphtho[2,3-a]carbazole-5,13-diones [39], which were also reported possessing cell growth inhibition against several tumourcelllines[40,41].Inspiredbyandasacontinuationof thesefindings,weenvisionedthattreating2,6-dibromocyclohexa-2,5-diene-1,4-dione(9)[42]withtwoequiv.ofindol-3ylic acid 6 would facilitate a two-side parallel cyclization of the dione 9 leading to cyclohexa-2,5-diene-1,4-dione-fused biscarbazole (11) in one step (Fig. 2). ...
    • ...Compounds 6 and 9 were prepared using the reported procedure [39,42]...
    • ...First, 2,6-dibromocyclohexa-2,5-diene-1,4-dione (9 )w as reacted stoichiometrically with indol-3-ylic acid 6 under our optimized conditions [35,39] by using 2 equiv...

    Shanghui Tuet al. Facile synthesis of indole- or benzofuran-fused benzo[a]carbazole-1,4-...

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