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Crystallization behaviour of poly(vinylidene fluoride)

Crystallization behaviour of poly(vinylidene fluoride),10.1016/S0014-3057(98)00242-0,European Polymer Journal,Paweł Sajkiewicz

Crystallization behaviour of poly(vinylidene fluoride)   (Citations: 13)
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Crystallization of poly(vinylidene fluoride) is investigated by calorimetry and wide-angle X-ray scattering. It is shown that in addition to α and γ crystallization at high temperatures, α crystallization occurs at low temperatures. It is probable that low temperature α crystallization occurs from the segments with high concentration of head-to-head defects which are unable to crystallize at high temperatures. The Hoffman–Weeks plot of α crystallites formed at high temperatures is affected by additional low temperature α crystallization. The change in slope of a Hoffman–Weeks plot for α crystallites, reported in several papers, occurs only in the structure additionally crystallized during cooling to room temperature. The equilibrium melting temperature of the α and γ form is determined from the Hoffman–Weeks plot.
Journal: European Polymer Journal - EUR POLYM J , vol. 35, no. 9, pp. 1581-1590, 1999
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