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Formation of palladium hydride nanoparticles in Pd/C catalyst as evidenced by in situ XAS data

Formation of palladium hydride nanoparticles in Pd/C catalyst as evidenced by in situ XAS data,10.1007/s11172-010-0002-x,Russian Chemical Bulletin,A.

Formation of palladium hydride nanoparticles in Pd/C catalyst as evidenced by in situ XAS data  
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X-ray absorption spectroscopy was used to investigate the formation of palladium hydride upon treatment of metallic Pd nanoparticles 0.9–2 nm in size supported on carbon-carbonaceous material SIB UNIT® with hydrogen. Nanoparticles with the size as small as 0.9 nm can still form hydride PdH. Changes in the chemical composition of gaseous medium cause a reversible transformation of metallic palladium nanoparticles to palladium hydride nanoparticles with tentative stoichiometry PdH0.6.
Journal: Russian Chemical Bulletin - RUSS CHEM BULL , vol. 58, no. 2, pp. 280-283, 2009
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