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The first heterometallic Mn–Ca cluster containing exclusively Mn(III) centers

The first heterometallic Mn–Ca cluster containing exclusively Mn(III) centers,10.1016/j.inoche.2010.10.025,Inorganic Chemistry Communications,Vasiliki

The first heterometallic Mn–Ca cluster containing exclusively Mn(III) centers  
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The reaction of Mn(ClO4)2·6H2O with Ca(prop)2 and Me-saOH2 in MeCN yields the heterometallic polymeric complex {[MnIII6Ca2O2(Me-saO)6(prop)6 (H2O)2].2MeCN.0.95H2O}n (1) (prop=propionate; Me-saOH2=2-hydroxyphenylethanone oxime). Complex 1 consists of hexanuclear centrosymmetric [MnIII6O2(Me-saO)6]2+ units bridged by propionate calcium [Ca2(prop)6]2− centrosymmetric dimers. Magnetic measurements show that the hexanuclear magnetic core has an S=4 ground state.
Journal: Inorganic Chemistry Communications - INORG CHEM COMMUN , vol. 14, no. 1, pp. 213-216, 2011
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