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Floating zone crystal growth and structural distortion of Pb 2V 3O 9

Floating zone crystal growth and structural distortion of Pb 2V 3O 9,10.1016/j.jcrysgro.2011.02.013,Journal of Crystal Growth,B. S. Conner,H. D. Zhou,

Floating zone crystal growth and structural distortion of Pb 2V 3O 9  
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Single crystals of the spin dimer compound Pb2V3O9 were grown for the first time by the floating zone method. Room temperature single-crystal X-ray diffraction measurements confirm their crystallinity and structure. The crystal growth process is discussed in detail and high temperature differential scanning calorimetry measurements that show a structural phase transition from a monoclinic to a triclinic unit cell at 759(1)K are presented.
Journal: Journal of Crystal Growth - J CRYST GROWTH , vol. 321, no. 1, pp. 120-123, 2011
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